13386 (v.3) Analytical Chemistry 114

Area:

Department of Applied Chemistry

Credits:

12.5

Contact Hours:

4.0

** The tuition pattern below provides details of the types of classes and their duration. This is to be used as a guide only. For more precise information please check your unit outline. **

Lecture:

1 x 1 Hours Weekly

Laboratory:

1 x 3 Hours Weekly

Syllabus:

Spectrophotometry. Electromagnetic radiation - energy levels, absorption of radiation. Quantitative applications of visible spectrophotometry - complexation reactions, indirect methods. The spectrophotometer - radiation sources, intensity control, wavelength control, sample holders, detectors. Lambert-Beer Law - linearity, deviations, sample calculations, two component systems. Introduction to chromatography - partition and adsorption processes. Column chromatography - solvent polarities (elutropic series). Paper chromatography - Rf value, two-dimensional paper chromatography. Thin layer chromatography (TLC) - advantages over paper, spot visualisation. Gel permeation. Ion exchange chromatography. Gas chromatography - basic relationships and instrumentation. Sampling procedures. Column efficiency - theoretical plates, resolution, HETP and effect of carrier gas flow rate methods of improving column efficiency. effect of temperature. The column - packed and capillary columns - liquid phase requirements, selection. Detectors - mode of operation, sensitivity, stability, selectivity and linearity of flame ionisation, thermal conductivity and electron capture detectors. Qualitative and quantitative analysis.

** To ensure that the most up-to-date information about unit references, texts and outcomes appears, they will be provided in your unit outline prior to commencement. **

Field of Education:

010500 Chemical Sciences (Narrow Grouping)

Funding Cluster:

08 - Engineering, Science, Surveying

SOLT (Online) Definitions*:

Informational
*Extent to which this unit or thesis utilises online information

Result Type:

Grade/Mark

Availability

Year	Location	Period	Internal	Partially Online Internal	Area External	Central External	Fully Online
2005	Bentley Campus	Semester 2	Y

Area External	refers to external course/units run by the School or Department or offered by research.
Central External	refers to external and online course/units run through the Curtin Bentley-based Distance Education Area
Partially Online Internal	refers to some (a portion of) learning provided by interacting with or downloading pre-packaged material from the Internet but with regular and ongoing participation with a face-to-face component retained. Excludes partially online internal course/units run through the Curtin Bentley-based Distance Education Area which remain Central External
Fully Online	refers to the main (larger portion of) mode of learning provided via Internet interaction (including the downloading of pre-packaged material on the Internet). Excludes online course/units run through the Curtin Bentley-based Distance Education Area which remain Central External