Courses Handbook 2008 - [ Archived ]

13386 (v.3) Analytical Chemistry 114


Area: Department of Applied Chemistry
Credits: 12.5
Contact Hours: 3.0
** The tuition pattern below provides details of the types of classes and their duration. This is to be used as a guide only. For more precise information please check your unit outline. **
Lecture: 1 x 1 Hours Weekly
Laboratory: 1 x 2 Hours Weekly
Syllabus: Spectrophotometry. Electromagnetic radiation: energy levels and absorption of radiation. Quantitative applications of visible spectrophotometry: complexation reactions and indirect methods. The spectrophotometer: radiation sources, intensity control, wavelength control, sample holders and detectors. Lambert-Beer Law: linearity, deviations, sample calculations and two component systems. Introduction to chromatography: partition and adsorption processes. Column chromatography: solvent polarities (eluotropic series). Paper chromatography: retardation factor (Rf) value and two-dimensional paper chromatography. Thin layer chromatography (TLC): advantages over paper and spot visualisation. Gel permeation. Ion exchange chromatography. Gas chromatography: basic relationships and instrumentation. Sampling procedures. Column efficiency: theoretical plates, resolution, HETP and effect of carrier gas flow rate methods of improving column efficiency. Effect of temperature. The column: packed and capillary columns, liquid phase requirements and selection. Detectors: mode of operation, sensitivity, stability, selectivity and linearity of flame ionisation, thermal conductivity and electron capture detectors. Qualitative and quantitative analysis.
** To ensure that the most up-to-date information about unit references, texts and outcomes appears, they will be provided in your unit outline prior to commencement. **
Field of Education: 010500 Chemical Sciences (Narrow Grouping)
SOLT (Online) Definitions*: Informational
*Extent to which this unit or thesis utilises online information
Result Type: Grade/Mark

Availability

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